Veidlapa Nr. M-3 (8)
Study Course Description
Qualitative Analysis
Course Code
LFK_014
Branch of Science
Basic medicine; Pharmaceutical Chemistry
ECTS
6.00
Target Audience
Pharmacy
LQF
Level 7
Study Type And Form
Full-Time
Study Course Implementer
Course Supervisor
Aija Trimdale-Deksne
Structure Unit Manager
Baiba Mauriņa
Structural Unit
Department of Applied Pharmacy
Contacts
Riga, 21 Consula Street, farmkk@rsu.lv, +371 67061544
About Study Course
Objective
Students must gain knowledge about the theoretical foundations of qualitative analytical chemistry and methods of qualitative analysis of inorganic substances and the use of these methods in practice.
Preliminary Knowledge
Mathematics (within the scope of the secondary school curriculum), General and Inorganic Chemistry (within the scope of the previous course "Inorganic Chemistry")
Learning Outcomes
Knowledge
1.Upon successful completion of the course: - knowledge of the chemistry of inorganic compounds will be strengthened; - methods of qualitative analysis of inorganic substances, their content and theoretical foundations will be mastered; - an understanding of the application possibilities of qualitative analytical methods will be gained.
Skills
1.At the end of the study course, the student shall be able to: - perform qualitative analysis of inorganic substances; - to be used in practice in the analysis of qualitative medicinal substances; - evaluate the results of the analysis.
Competences
1.As a result of the successful study course, the student will be able to: - recommend and justify the best qualitative methods of analysis for the analysis of inorganic chemicals; - qualitatively detect the presence of impurities in substances.
Assessment
Individual work
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Title
|
% from total grade
|
Grade
|
|---|---|---|
|
1.
Individual work |
-
|
-
|
|
Independent work on the course shall include: - hearing and learning video recordings of lectures; - preparation of minutes of laboratory work; - performance of self-control tasks on colloquia topics; - preparation for course seminars and examinations after the programme specified in e-studies; - completion of the study course evaluation questionnaire. |
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Examination
|
Title
|
% from total grade
|
Grade
|
|---|---|---|
|
1.
Examination |
-
|
10 points
|
|
Summary assessment work: - three colloquia and exam work, including the correct answer selection tasks, matching tasks, chemical response, situation analysis tasks. Evaluation on a grade in accordance with the provisions of RSU academic Regulations. - regular evaluation work in 3 practical classes. In classes between colloquiums, earned points are expressed as a percentage and represent 10% of the total score of colloquia. - final assessment of the course is cumulative (50% consists of the assessment obtained during the course and 50% of the assessment obtained during the exam work). |
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Study Course Theme Plan
FULL-TIME
Part 1
-
Lecture
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
Off site
|
Video
|
2
|
Topics
|
Lecture: theoretical basics of qualitative analysis
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
An introductory lesson.
Entrance colloquium on inorganic chemistry course.
|
-
Lecture
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
Off site
|
Video
|
2
|
Topics
|
Lecture: Buffer and heterogeneous systems in Analytical Chemistry
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Cation analysis - qualitative reactions
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Laboratory work: Cationic analysis — Cationic mixture analysis of analytical groups 1 to 3
Seminar: solutions, systematic and selective analysis, reaction sensitivity
Test: qualitative demonstration of cations of analytical groups 1 to 3.
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Seminar: Protolites. Buffer systems.
colloquia 1: theoretical basics of qualitative analysis, qualitative demonstration of cations of analytical groups 1-3.
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Laboratory work. Cation analysis — Canyon mixture analysis of analytical groups 4 to 6
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Seminar: heterogeneous systems in chemical analysis
colloquia 2: qualitative demonstration of protolites, buffer systems, cations of analytical groups 4-6
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Selective analysis of inorganic salts.
Colloquium No. 2.
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Anion mixture analysis.
Test: qualitative reactions of anions.
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Cation and anion mixture analysis.
Seminar: heterogeneous systems in chemical analysis.
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Laboratory work. Analysis of the mixture of cations and anions (continuation)
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Theoretical qualitative analysis of inorganic salts.
|
-
Class/Seminar
|
Modality
|
Location
|
Contact hours
|
|---|---|---|
|
On site
|
Laboratory
|
5
|
Topics
|
Seminar: Independent work with Literature
|
Total ECTS (Creditpoints):
6.00
Contact hours:
64 Academic Hours
Final Examination:
Exam (Written)
Bibliography
Required Reading
1.
Jansons E. Analītiskās ķīmijas teorētiskie pamati. Rīga: LU Akadēmiskais apgāds, 2006. (akceptējams izdevums)
2.
Skoog D.A. West D.M. Analytical Chemistry. An Introduction. 10th edition. Philadelphia: Saunders College Publishing, 2022.Suitable for English stream
Additional Reading
1.
Moller T. Kleinberg J. Castillion M.E. et al. Chemistry with Inorganic Qualitative Analysis. 2nd edition. New York: Academic Press, 1984.Suitable for English stream
Other Information Sources
1.
Harris D.C. Qualitative Chemical Analysis. 7th edition. New York: W.Freemanand Company, 2007.Suitable for English stream
2.
Harvey D. Modern Analytical Chemistry. New York: McGraw Hill Companies, 2000.Suitable for English stream
3.
Valcárcel M. Principles of Analytical Chemistry. Springer, New York: Springer, 2000.Suitable for English stream